Efek NaOH pada Pembentukan Nano ZnO Metode Hidrotermal
DOI:
https://doi.org/10.23960/jemit.v2i3.146Keywords:
ZnO, NaOH, HidrotermalAbstract
Hydrothermal methods have been developed for the manufacture of ZnO. This study aims to find out the effects of variation on the chemical composition and structure of nanoZnO, the nanoZnO phase formed and the nanoZnO particle size formed. The NaOH variation used is 1; 2; 3; and 4 grams. The characteristics used are X-Ray Diffactions (XRD) and Scanning Electron Microscopy (SEM). The XRD characterization results show that the diffraction peaks correspond to standard databases and show wurtzite phases with hexagon structures. The results of SEM characterization showed that the mean measurement of ZnO particles and the error value in the 1 gram variation was 67 ± 3 nm, while the 3 gram variation was 76 ± 6 nm.
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References
Anonymous. An Overview On Uses Of Zinc Oxide Nanoparticles.
Albertson, J., Abrahams, S. C. and Kvick, A. (1989). Section B: Structural Science. Acta Crystallographica.
Alfarisa, S. (2018). Sintesis Struktur Mikro - Nano ZnO Menggunakan Metode Hidrotermal Sederhana Bersuhu Rendah. July, 23–26.
Council, S. P. (2007). Nanotechnology White Paper. February.
Darajat, S., Aziz, H., & Alif, A. (2015). Seng Oksida (ZnO) Sebagai Fotokatalis Pada Proses Degradasi Senyawa Biru Metilen. Jurnal Riset Kimia, 1(2), 179. https://doi.org/10.25077/jrk.v1i2.72
Dengyuan, H. and Xiaoping, Z. (2005). An Overview on Uses of Zinc Oxide Nanoparticles. Rf Magnetron Sputtering.
Hong, R. Y., Feng, B., Chen, L. L., Liu, G. H., Li, H. Z., Zheng, Y., & Wei, D. G. (2008). Synthesis, characterization and MRI application of dextran-coated Fe3O4 magnetic nanoparticles. Biochemical Engineering Journal, 42(3), 290–300. https://doi.org/10.1016/j.bej.2008.07.009
Hossary, F. M. El, El-rahman, A. M. A., & Abdelhamidshahat, M. (2018). Low Hydrothermal Temperature Synthesis and Characterization of ZnO Low Hydrothermal Temperature Synthesis and Characterization of ZnO Nanoparticles. May.
Khan, F. M., Hamedullah, M., Ejaz, A. H. A., Lohani, A. M. B., Khan, R. H., Alam, M. M., dan Khan, W. (2014). Nanopartikel ZnO Berbentuk Bunga yang Disintesis dengan Pendekatan Baru pada Suhu Hampir Ruang dengan Sifat Antibakteri dan Antijamur. Journal International Nano Medichine, 9, 853–864.
Lauterwasser, C. (2006). Opportunities and risks of Nanotechnologies. Allianz AC.
Lee, S., Jeong, S., Kim, D., Hwang, S., Jeon, M., & Moon, J. (2008). ZnO nanoparticles with controlled shapes and sizes prepared using a simple polyol synthesis. Superlattices and Microstructures, 43(4), 330–339. https://doi.org/10.1016/j.spmi.2008.01.004
Morey, G. W. (1953). Hydrothermal Synthesis. Journal of the American Ceramic Society, 36(9), 279–285. https://doi.org/10.1111/j.1151-2916.1953.tb12883.x
Nithiya, P., Chakra, C. H. S., & Ashok, C. (2015). Synthesis of TiO2 and ZnO Nanoparticles by Facile Polyol Method for the Assessment of Possible Agents for Seed Germination. Materials Today: Proceedings, 2(9), 4483–4488. https://doi.org/10.1016/j.matpr.2015.10.056
Ortiz-Landeros, J., Gómez-Yáñez, C., López-Juárez, R., Dávalos-Velasco, I., & Pfeiffer, H. (2012). Synthesis of advanced ceramics by hydrothermal crystallization and modified related methods. Journal of Advanced Ceramics, 1(3), 204–220. https://doi.org/10.1007/s40145-012-0022-0
Sari, R. N., Saridewi, N., & Shofwatunnisa, S. (2017). Biosynthesis and Characterization of ZnO Nanoparticles with Extract of Green Seaweed Caulerpa sp. Jurnal Perikanan Universitas Gadjah Mada, 19(1), 17. https://doi.org/10.22146/jfs.24488
Sawada, H., Wang, R., & Sleight, A. W. (1996). An electron density residual study of zinc oxide. Journal of Solid State Chemistry, 122(1), 148–150. https://doi.org/10.1006/jssc.1996.0095
Ui, F. T. (2011). Universitas Indonesia Karakterisasi Nanopartikel ZnO Hasil Sintesis Dengan Metode Presipitasi dan Perlakuan Pra- Depok.
Zhai, Y., Hunting, E. R., Wouterse, M., Peijnenburg, W. J. G. M., & Vijver, M. G. (2017). Importance of exposure dynamics of metal-based nano-ZnO, -Cu and -Pb governing the metabolic potential of soil bacterial communities. Ecotoxicology and Environmental Safety, 145, 349–358. https://doi.org/10.1016/j.ecoenv.2017.07.031
Zhang, Q., Yu, K., Bai, W., Wang, Q., Xu, F., Zhu, Z., Dai, N., & Sun, Y. (2007). Synthesis, optical and field emission properties of three different ZnO nanostructures. Materials Letters, 61(18), 3890–3892. https://doi.org/10.1016/j.matlet.2006.12.064
